Sahih Bukhari | Volume 6 | Hadith Number 386

Narrated by Abdullah
The first Sura in which a prostration was mentioned, was Sura An-Najm (The Star). Allah's Apostle prostrated (while reciting it), and everybody behind him prostrated except

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a man whom I saw taking a hand-full of dust in his hand and prostrated on it. Later I saw that man killed as an infidel, and he was Umaiya bin Khalaf.